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Figure 13.23. Time dependency of relative strain of semi-IPN lms under alternating switching on and off of (a) UV, (b) UV+visible light, and (c) visible. Source: Kim et al., 2005a,b. Reprinted with permission.

21 to the amminates or hydrates of salts can be crystallized from these solutions The solutions are blue (absorb at 7000 cm"1, corresponding to the s->p electron transition) and paramagnetic Paramagnetic resonance measurements indicate that cavities in the liquid with dimensions of about 03 nm contain free electrons Compared with aqueous salt solutions, these metal solutions have about 105 times larger molar conductivity, indicating electronic conductivity Thus, the metals in solution are dissociated to yield solvated cations M+ and electrons e~ (also solvated) More concentrated solutions also contain species such as M + e~, M2 and Me" The stability of these solutions is low because of the formation, for example, of alkali metal amides in solutions of alkali metals in liquid ammonia A form of solvation also occurs in ionic solvents, but coulombic interactions predominate.

The solvent structure can be conceived as resulting from the penetration of two sublattices cationic and anionic The cations of the dissolved salt are then scattered throughout the cationic sublattice and the anions in the anionic sublattice If the dissolved salt and the solvent have a common anion, for example, then the cations are scattered throughout the cationic sublattice and the anionic lattice remains almost unaffected Let us assume that only one kind of foreign ion, a cation or an anion, is introduced into ionic solvents (while the electroneutrality condition is maintained) If the cation of the dissolved salt has a larger charge than the solvent cation, then vacancies must be scattered throughout the cationic sublattice so that the distribution of electric charge remains neutral An example of a more complicated situation is the formation of Na+ and A1C14~ ions in an equimolar melt of A1C13 + NaCl.

The aggregation dissociation mechanism (Kim et al, 2005a,c) tentatively proposed to explain the modulus change of the lm under the alternating switching on and off of the UV irradiation is inadequate to account for the systems driven by the visible light Under visible light irradiation, the lm exhibited a behavior similar to that under UV irradiation Endo and coworkers proposed a dynamic mechanism (Kim et al, 2005b) to explain this phenomenon The azobenzene ligands under light irradiation change their conformation (trans or cis) dynamically at any moment In other words, azobenzene moieties resonate to the incident light and the energy from irradiation is transformed into the vibratory motion of the excited azobenzene The trans-azobenzene can be excited by UV light and the cis-azobenzene can be excited by visible light.

Product (Chassis)

If the mixture contains a small excess of A1C13 over the stoichiometric amount, then A12C17~ ions are also present If Cu+ ions are then dissolved in the melt (as CuCl), they remain free and are scattered throughout the cationic sublattice However, in the presence of a small excess of NaCl, the anionic sublattice contains a corresponding excess of Cl~ with which the Cu+ ions form the CuCl2" complex which is spread throughout the anionic sublattice Three types of methods are used to study solvation in molecular solvents These are primarily the methods commonly used in studying the structures of molecules However, optical spectroscopy (IR and Raman) yields results that are difficult to interpret from the point of view of solvation and are thus not often used to measure solvation numbers NMR is more successful, as the chemical shifts are chiefly affected by solvation.

Thus both types of irradiation can trigger the vibratory motion, which disturbs the local packing of the polymer chain and creates local free volume, resulting in a decrease in the modulus and elongation of the lm When the light is switched off, the azobenzene moieties cannot harvest photo energy for subsequent resonating Thus the local free volume in the matrix disappears and the initial modulus is recovered completely This mechanism is evidenced by several other studies One example is that the frequent photoisomerization of azobenzene moieties could induce the softening of polymer lms because of the light-induced free volume formation under UV and visible irradiation (Mechau et al, 2005, 2002) Macroscopic deformation is a collective behavior of the numerous azobenzene ligands incorporated into the material It is much easier to detect experimentally than molecular-level deformation.

Yes (Optimal application)

Measurement of solvation-dependent kinetic quantities is often used {electrolytic mobility, diffusion coefficients, etc) These methods supply data on the region in the immediate vicinity of the ion, ie the primary solvation sphere, closely connected to the ion and moving together with it By means of the third type of methods some static quantities (entropy and compressibility as well as some non-thermodynamic quantities such as the dielectric constant) are measured These methods also pertain to the secondary solvatibff sphere, in which the solvent structure is affected by the presence of ions, but the.