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Novel wormlike nanostructure self assembled in a well de ned liquid crystalline diblock copolymer with azobenzene moieties Macromol Rapid Commun 28:927 931..

181 It follows from the additivity of affinities, AG2_() = AG2_i AG^Q, that (z+,2 - z+>1)E _i = z + , 2 ^_ 0 - z+>1 _o (3.2.24)

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Yu HF, Shishido A, Iyoda T, Ikeda T. 2009. Effect of recording time on grating formation and enhancement in an amphiphilic diblock liquid crystalline copolymer. Mol Cryst Liq Cryst 498:29 39. Yu Y, Nakano M, Ikeda T. 2003. Directed bending of a polymer lm by light. Nature 425:145 145. Zhang Y, Cheng Z, Chen X, Zhang W, Wu J, Zhu J, Zhu X. 2007. Synthesis and photoresponsive behaviors of well de ned azobenzene containing polymers via RAFT polymerization. Macromolecules 40:4809 4817.

Conclusion Appendix A Vendor and Product Information Appendix B Standards and Specifications Glossary Bibliography Index

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This relationship (sometimes called Luther's law) for the transfer of several electrons permits us to calculate one redox potential if the others are known. Obviously, this is an analogy of the Hess law in thermodynamics. Equation (3.2.24) is not restricted to the case where the lowest oxidation state is a metal. Consider the reactions A + e<^B and B + e<= C (3.2.25)

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In general, the de nition of stimuli-responsive materials is that material properties (color, volume, adsorption, refractive index, stress, etc.) undergo predictable changes in response to external stimuli, such as light, heat, and pH. Because of their intelligent response, such materials are of potential interest for applications in micro uidics, microvalves, controlled drug release, sensors, optical switches, photomemories, light-driven displays, optical storage, and optomechanical actuation. Azobenzene-containing materials are some of the most commonly used stimuli-responsive materials because of their well-known responses to light and heat (Natansohn, 1999; Rau, 1990b; Kumar and Neckers, 1989). Ultraviolet (UV) irradiation of the trans isomer causes its transformation to the cis isomer. Removal of the UV light, heating, or irradiation with a longer wavelength light switches the system back to the trans form. Trans2cis isomerization of azobenzene moieties changes not only the molecular dimension, but also the dipole moment (0.5 3.1 Debye). Most of the work on photoresponsive azobenzene-containing materials is based on polymer matrices. Numerous chemistries have been utilized to graft azobenzene ligands to various polymer chains. The azobenzene chromophores transfer light energy into conformational changes upon photoirradiation, which can be used to control chemical and physical properties of the materials, such as viscosity, conductivity, pH, solubility, wettability, permeability, transport properties, mechanical properties, and structural properties. Azobenzene ligands have also been incorporated into inorganic silica matrices. The robust inorganic silica framework does have some advantages in terms

274 275 331 263 357 361

The sum of these reactions yields a reaction termed disproportionation: aB (3.2.26)

Smart Light Responsive Materials. Edited by Yue Zhao and Tomiki Ikeda Copyright r 2009 John Wiley & Sons, Inc.

where K is the disproportionation constant. An inert electrode immersed in a solution containing species A, B and C will attain a potential corresponding to both of equilibria (3.2.25): E = A,B + ^ l n ^ = Elc + ^ l n ^ (3.2.27) F aB F ac If the system initially contains only form C with concentration c0, to which the oxidant is added, then the overall degree of oxidation is (3 = (2[A] + [B])/c0. If activities are set equal to concentrations, then the potential E can be expressed in terms of j8:

So many people helped to make this book what it is; it is difficult to name them all First, I want to thank Anne Skamarock for her collaboration, partnership, and long hours in researching, analyzing, debating, and co-writing this book and for helping me to keep my sanity throughout the project Without Anne, this book would have been possible, but not nearly as good and certainly not as much fun Second, I want to thank Winston Bumpus at Dell, because when I was deciding whether or not to say yes to Wiley and write this book, his sage answer was Oh, go do it, and he convinced me I would be glad when it was done (and he offered his help and support) Thanks also for his great work on the management and standards issues and chapters and for connecting me with Prakash and other helpful people at Dell.

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